Sigma-Aldrich 69479 N-Methyl-N-(trimethylsilyl)trifluoroacetamide for GC derivatization, LiChropur™, ≥98.5% 25 mL
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Marka
Stok Kodu
LB.SA.69479-25ML
Kısa Bilgi
ynonym(s): N-Trimethylsilyl-N-methyl trifluoroacetamide, MSTFA Linear Formula: CF3CON(CH3)Si(CH3)3 CAS Number: 24589-78-4 Molecular Weight: 199.25 Beilstein: 1941550 EC Number: 246-331-6 MDL number: MFCD00000411 PubChem Substance ID: 329761689 NACRES: NA.22
| Sigma-Aldrich 69479 N-Methyl-N-(trimethylsilyl)trifluoroacetamide |
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Synonym(s): N-Trimethylsilyl-N-methyl trifluoroacetamide, MSTFA
Linear Formula: CF3CON(CH3)Si(CH3)3
CAS Number: 24589-78-4
Molecular Weight: 199.25
Beilstein: 1941550
EC Number: 246-331-6
MDL number: MFCD00000411
PubChem Substance ID: 329761689
NACRES: NA.22
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PROPERTIES
grade for GC derivatization
Quality Level 100
vapor density >1 (vs air)
vapor pressure 8.8 mmHg ( 27 °C)
assay ≥98.5% (GC) ≥98.5%
form liquid
quality LiChropur™
reaction suitability reagent type: derivatization reagent, reaction type: Silylations
technique(s) gas chromatography (GC): suitable
refractive index n20/D 1.38 (lit.) n20/D 1.380
bp 130-132 °C (lit.)
density 1.075 g/mL at 25 °C (lit.)
storage temp. 2-8°C
SMILES string CN(C(=O)C(F)(F)F)[Si](C)(C)C
InChI 1S/C6H12F3NOSi/c1-10(12(2,3)4)5(11)6(7,8)9/h1-4H3
InChI key MSPCIZMDDUQPGJ-UHFFFAOYSA-N
DESCRIPTION
General description
N-Methyl-N-(trimethylsilyl)trifluoroacetamide (MSTFA) is a silylating reagent.[1]
Application
Learn more in the Product Information MSTFA may be used in silylation procedure to detemine steroid hormones 17α-ethinylestradiol (EE2) and estrone using GC-MS. MSTFA along with Trimethylsilyl chloride (TMCS) in eithyl acetate, acetonitrile and dichloromethane solvents leads to formation of trimethylsilyl (TMS) and tert-butyldimethylsilyl (TBS) derivatives.[1] Suitable for the derivatization of amines, amino acids, carboxyl, hydroxyamines, indolalkylamine, n-nitrosoamino acids, nucleosides, phenolalkylamines, serotonin and tryptamine.
Packaging
1, 1, 5, 25 mL
Other Notes
Powerful silylating agent[2][3][4][5] Reagent for N-acetyl-N, trifluoroacetyl, trimethylsilyl, N-trimethylsilyl-N-trifluoroacetyl, and O-trimethylsilyl (TMS)
Legal Information
LiChropur is a trademark of Merck KGaA, Darmstadt, Germany
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